Difference between revisions of "Liquid-liquid extraction - 2014"
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| video_download_link_MP4_size = 468 M | | video_download_link_MP4_size = 468 M | ||
| video_notes1 = | | video_notes1 = | ||
| video_download_link2_MP4 = http://learnche.mcmaster.ca/media/2014-4M3-Class- | | video_download_link2_MP4 = http://learnche.mcmaster.ca/media/2014-4M3-Class-10A.mp4 | ||
| video_download_link2_MP4_size = M | | video_download_link2_MP4_size = M | ||
| video_notes2 = | | video_notes2 = | ||
| video_download_link3_MP4 = http://learnche.mcmaster.ca/media/2014-4M3-Class- | | video_download_link3_MP4 = http://learnche.mcmaster.ca/media/2014-4M3-Class-10B.mp4 | ||
| video_download_link3_MP4_size = | | video_download_link3_MP4_size = M | ||
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| video_download_link4_MP4 = http://learnche.mcmaster.ca/media/2014-4M3-Class- | | video_download_link4_MP4 = http://learnche.mcmaster.ca/media/2014-4M3-Class-10C.mp4 | ||
| video_download_link4_MP4_size = | | video_download_link4_MP4_size = M | ||
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[[Media:2014-4M3-Liquid-Liquid-Extraction.pdf|Slides]] | [[Media:2014-4M3-Liquid-Liquid-Extraction.pdf|Slides]] | ||
| [http://learnche.mcmaster.ca/media/2014-4M3-Class-09B.mp4 Video] | | [http://learnche.mcmaster.ca/media/2014-4M3-Class-09B.mp4 Video] | ||
| [http://learnche.mcmaster.ca/media/2014-4M3-Class- | | [http://learnche.mcmaster.ca/media/2014-4M3-Class-09B.mp3 Audio] | ||
|align="left" colspan="1"| | |align="left" colspan="1"| | ||
A comprehensive article on [http://learnche.mcmaster.ca/media/mcmaster/Bailes-Hanson-Hughes--Liquid-liquid-extraction.pdf liquid-liquid extraction] which describes the various units available. | A comprehensive article on [http://learnche.mcmaster.ca/media/mcmaster/Bailes-Hanson-Hughes--Liquid-liquid-extraction.pdf liquid-liquid extraction] which describes the various units available. | ||
|- | |- | ||
| 04 November | |||
| 10A | |||
| align="left" colspan="1"| | |||
Liquid liquid extraction theory and calculations | |||
| align="left" colspan="1"| | |||
[[Media:2014-4M3-Liquid-Liquid-Extraction.pdf|Slides]] | |||
| [http://learnche.mcmaster.ca/media/2014-4M3-Class-10A.mp4 Video] | |||
| [http://learnche.mcmaster.ca/media/2014-4M3-Class-10A.mp3 Audio] | |||
|align="left" colspan="1"| | |||
* The flowsheet for separating acetic acid from water using ethyl acetate solvent. This flowsheet has the mass flow rates, to help contrast it to distillation. | |||
:[[Image:Acetic-acid-water-ethyl-acetate-flowsheet-Seader-3ed-p300.jpg|300px]] <span style="color:#8822AA">''click to enlarge''</span> [reference: Seader ''et al.'', p300] | |||
* The [[Media:Seader-ternary-example-base.pdf|ternary diagram used in today's class]]. Download and print it out for practice problems. | |||
|} | |} | ||
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These first 3 readings seem old, but they are still relevant. For example, the same principles are used in modern bioseparations. | These first 3 readings seem old, but they are still relevant. For example, the same principles are used in modern bioseparations. | ||
* A [http://learnche.mcmaster.ca/media/mcmaster/Hanson--Solvent-extraction.pdf reading on solvent extraction principles] | |||
# A [http://learnche.mcmaster.ca/media/mcmaster/Hanson--Solvent-extraction.pdf reading on solvent extraction principles] | # A [http://learnche.mcmaster.ca/media/mcmaster/Hanson--Solvent-extraction.pdf reading on solvent extraction principles] | ||
# A general article on [http://learnche.mcmaster.ca/media/mcmaster/Reissinger-Schroter--Liquid-liquid-extractors.pdf liquid liquid extractors]. | # A general article on [http://learnche.mcmaster.ca/media/mcmaster/Reissinger-Schroter--Liquid-liquid-extractors.pdf liquid liquid extractors]. | ||
# An interesting [http://learnche.mcmaster.ca/media/mcmaster/Moore--Using-principles-of-inherent-safety-in-design-of-hydrometallurgical-solvent-extraction-plants.pdf reading on safety in liquid-liquid extraction plants]: a further reason for counter-current operations to minimize solvent use. | # An interesting [http://learnche.mcmaster.ca/media/mcmaster/Moore--Using-principles-of-inherent-safety-in-design-of-hydrometallurgical-solvent-extraction-plants.pdf reading on safety in liquid-liquid extraction plants]: a further reason for counter-current operations to minimize solvent use. | ||
# Here's [http://webpages.sdsmt.edu/~ddixon/CBE417_Lec_23_LLE_Draft_3-print.pdf another instructor's slides] on the same topic - sometimes a different point of view helps to understand. | # Here's [http://webpages.sdsmt.edu/~ddixon/CBE417_Lec_23_LLE_Draft_3-print.pdf another instructor's slides] on the same topic - sometimes a different point of view helps to understand. | ||
--> | --> | ||
Revision as of 12:47, 4 November 2014
| Class date(s): | 29 October 2014 | ||||
| |||||
References
Please use these references to read ahead, or for extra background reading on liquid-liquid extraction. In alphabetical order:
- Ghosh, R. "Principles of Bioseparations Engineering", Chapter 7, McMaster (reserve)
- Geankoplis, C.J. "Transport Processes and Separation Process Principles", Chapter 12 in 3rd and 4th edition, McMaster Libraries (reserve)
- Perry's Chemical Engineers' Handbook, Chapter 15, Direct link (McMaster subscription)
- Richardson and Harker, "Chemical Engineering, Volume 2", 5th edition, Chapter 13 ebook
- Schweitzer, "Handbook of Separation Techniques for Chemical Engineers", Chapter 1.9, McMaster library
- Seader, Henley and Roper, "Separation Process Principles", Chapter 8 in 2nd and 3rd edition McMaster Libraries (reserve)
| Date | Class number | Topic | Slides for class | Video and audio files | References and Notes | |
|---|---|---|---|---|---|---|
| 29 October | 09B |
Liquid liquid extraction overview |
Video | Audio |
A comprehensive article on liquid-liquid extraction which describes the various units available. | |
| 04 November | 10A |
Liquid liquid extraction theory and calculations |
Video | Audio |
| |
