Difference between revisions of "Liquid-liquid extraction - 2012"

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| vimeoID2 = 52160867
| vimeoID2 = 52160867
| vimeoID3 = 52235395
| vimeoID3 = 52235395
| vimeoID4 =
| vimeoID4 = 52479254
| vimeoID5 =
| vimeoID5 =
| vimeoID6 =
| vimeoID6 =
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| video_download_link3_MP4_size = 127 M
| video_download_link3_MP4_size = 127 M
| video_notes3 =
| video_notes3 =
| video_download_link4_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-09A.mp4
| video_download_link4_MP4_size = 119 M
| video_notes4 =
}}__TOC__
}}__TOC__
We start this section by looking at liquid-liquid extraction.
We start this section by looking at liquid-liquid extraction.
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=== 23 Oct 2012 (08A) ===
=== 23 Oct 2012 (08A) ===
* [[Media:2012-4M3-class-08A.pdf | Slides for class]] (print slides 4 to 11)
* [[Media:2012-4M3-class-08A.pdf | Slides for class]] (print slides 4 to 11)
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08A.mp4 video] recording of the class
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08A.mp4 video] recording of the class.


=== 25 Oct 2012 (08B) ===
=== 25 Oct 2012 (08B) ===
* [[Media:2012-4M3-class-08B.pdf | Slides for class]] (print slides 9 to 28) are new/revised. Please make minor updates to your previous printout, or reprint slides of interest.
* [[Media:2012-4M3-class-08B.pdf | Slides for class]] (print slides 9 to 28) are new/revised. Please make minor updates to your previous printout, or reprint slides of interest.
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08B.mp4 video] recording of the class
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08B.mp4 video] recording of the class.


=== 26 Oct 2012 (08C) ===
=== 26 Oct 2012 (08C) ===
* [[Media:2012-4M3-class-08C-with-solutions.pdf | Slides for class]] (print slides 24 to 35). Print slides 29, 30, 32 and 35 on separate, large pages. The slide on selecting a solvent was updated with the full solution.
* [[Media:2012-4M3-class-08C-with-solutions.pdf | Slides for class]] (print slides 24 to 35). Print slides 29, 30, 32 and 35 on separate, large pages. The slide on selecting a solvent was updated with the full solution.
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08C.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08C.mp4 video] recording of the class
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08C.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08C.mp4 video] recording of the class.
* Three photos of the board during class
* Three photos of the board during class
:[[Image:Board-26-Oct-2012-A.jpg|400px]] ''click to enlarge''  
:[[Image:Board-26-Oct-2012-A.jpg|400px]] ''click to enlarge''  
Line 67: Line 70:
We will wrap up the section on liquid-liquid extraction.
We will wrap up the section on liquid-liquid extraction.
* [[Media:2012-4M3-class-08D.pdf | Slides for class]] (print slides 36 to 49)
* [[Media:2012-4M3-class-08D.pdf | Slides for class]] (print slides 36 to 49)
<!--* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08A.mp4 video] recording of the class -->
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-09A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-09A.mp4 video] recording of the class.
* Photo of the board during class
:[[Image:Board-30-Oct-2012.jpg|400px]] ''click to enlarge''

Revision as of 17:03, 30 October 2012

Class date(s): 23 to 26 October 2012
Download video: Link [102 M]

Download video: Link [123 M]

Download video: Link [127 M]

Download video: Link [119 M]

We start this section by looking at liquid-liquid extraction.

References

Please use these references to read ahead, or for extra background reading on liquid-liquid extraction. In alphabetical order:

  • Ghosh, R. "Principles of Bioseparations Engineering", Chapter 7, McMaster (reserve)
  • Geankoplis, C.J. "Transport Processes and Separation Process Principles", Chapter 12 in 3rd and 4th edition, McMaster Libraries (reserve)
  • Perry's Chemical Engineers' Handbook, Chapter 15, Direct link (McMaster subscription)
  • Richardson and Harker, "Chemical Engineering, Volume 2", 5th edition, Chapter 13 ebook
  • Schweitzer, "Handbook of Separation Techniques for Chemical Engineers", Chapter 1.9, McMaster library
  • Seader, Henley and Roper, "Separation Process Principles", Chapter 8 in 2nd and 3rd edition McMaster Libraries (reserve)

Interesting applications / Enrichment materials

  • An article on liquid-liquid extraction which describes the various units available.
  • The flowsheet for separating acetic acid from water using ethyl acetate solvent. This flowsheet has the mass flow rates, to help contrast it to distillation.
Acetic-acid-water-ethyl-acetate-flowsheet-Seader-3ed-p300.jpg
click to enlarge

Week 8

23 Oct 2012 (08A)

25 Oct 2012 (08B)

  • Slides for class (print slides 9 to 28) are new/revised. Please make minor updates to your previous printout, or reprint slides of interest.
  • Audio and video recording of the class.

26 Oct 2012 (08C)

  • Slides for class (print slides 24 to 35). Print slides 29, 30, 32 and 35 on separate, large pages. The slide on selecting a solvent was updated with the full solution.
  • Audio and video recording of the class.
  • Three photos of the board during class
Board-26-Oct-2012-A.jpg click to enlarge
Board-26-Oct-2012-B.jpg click to enlarge
Board-26-Oct-2012-C.jpg click to enlarge

Week 9

30 Oct 2012 (08A)

We will wrap up the section on liquid-liquid extraction.

Board-30-Oct-2012.jpg click to enlarge