Difference between revisions of "Liquid-liquid extraction - 2012"

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| date = 23 to 26 October 2012
| date = 23 to 26 October 2012
| dates_alt_text =  
| dates_alt_text =  
| vimeoID1 =  
| vimeoID1 = 52046106
| vimeoID2 =
| vimeoID2 = 52160867
| vimeoID3 =  
| vimeoID3 = 52235395
| vimeoID4 =
| vimeoID4 = 52479254
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| vimeoID5 = 52633575
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| assignment_solutions =  
| assignment_solutions =  
| video_download_link_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-08A.mp4
| video_download_link_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-08A.mp4
| video_download_link_MP4_size = 116 M
| video_download_link_MP4_size = 102 M
| video_notes1 =
| video_notes1 =
| video_download_link2_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-08B.mp4
| video_download_link2_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-08B.mp4
| video_download_link2_MP4_size = 104 M
| video_download_link2_MP4_size = 123 M
| video_notes2 =
| video_notes2 =
| video_download_link3_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-08C.mp4
| video_download_link3_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-08C.mp4
| video_download_link3_MP4_size = 44 M
| video_download_link3_MP4_size = 127 M
| video_notes3 =
| video_notes3 =
| video_download_link4_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-09A.mp4
| video_download_link4_MP4_size = 119 M
| video_notes4 =
| video_download_link5_MP4 = http://learnche.mcmaster.ca/media/4M3-2012-09B.mp4
| video_download_link5_MP4_size = 119 M
| video_notes5 =
}}__TOC__
}}__TOC__
We start this section by looking at liquid-liquid extraction.


== References ==
== References ==
''Coming soon''
Please use these references to read ahead, or for extra background reading on liquid-liquid extraction. In alphabetical order:
 
* Ghosh, R. "Principles of Bioseparations Engineering", Chapter 7, [http://catalogue.mcmaster.ca/catalogue/Record/1405538 McMaster] (reserve)
* Geankoplis, C.J. "Transport Processes and Separation Process Principles", Chapter 12 in 3rd and 4th edition, [http://catalogue.mcmaster.ca/catalogue/Record/1219775 McMaster Libraries] (reserve)
* Perry's Chemical Engineers' Handbook, Chapter 15, [http://accessengineeringlibrary.com/browse/perrys-chemical-engineers-handbook-eighth-edition/p200139d899720_36001 Direct link] (McMaster subscription)
* Richardson and Harker, "Chemical Engineering, Volume 2", 5th edition, Chapter 13 [http://books.google.ca/books/about/Coulson_and_Richardson_s_Chemical_Engine.html?id=ottGCe1CDUoC ebook]
* Schweitzer, "Handbook of Separation Techniques for Chemical Engineers", Chapter 1.9, [http://catalogue.mcmaster.ca/catalogue/Record/1156427 McMaster library]
* Seader, Henley and Roper, "Separation Process Principles", Chapter 8 in 2nd and 3rd edition [http://catalogue.mcmaster.ca/catalogue/Record/1270236 McMaster Libraries] (reserve)
 
== Interesting applications / Enrichment materials ==
 
* An article on [http://learnche.mcmaster.ca/media/mcmaster/Bailes-Liquid-liquid-extraction.pdf liquid-liquid extraction] which describes the various units available.
* An article on [http://learnche.mcmaster.ca/media/mcmaster/Reissinger-Schroter--Selection-criteria-for-liquid-liquid-extraction-systems.pdf how to select among various liquid-liquid extraction units]
* The flowsheet for separating acetic acid from water using ethyl acetate solvent. This flowsheet has the mass flow rates, to help contrast it to distillation.
:[[Image:Acetic-acid-water-ethyl-acetate-flowsheet-Seader-3ed-p300.jpg|300px]] <span style="color:#8822AA">''click to enlarge''</span>


<!-- == Interesting applications / Enrichment materials == -->
== Week 8 ==
== Week 8 ==


=== 23 Oct 2012 (08A) ===
=== 23 Oct 2012 (08A) ===
Slides of class: will be posted on 22 October.
* [[Media:2012-4M3-class-08E.pdf | Slides for class]]
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08A.mp4 video] recording of the class.
 
=== 25 Oct 2012 (08B) ===
* [[Media:2012-4M3-class-08E.pdf | Slides for class]]
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08B.mp4 video] recording of the class.
 
=== 26 Oct 2012 (08C) ===
* [[Media:2012-4M3-class-08E.pdf| Slides for class]]
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-08C.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-08C.mp4 video] recording of the class.
* Three photos of the board during class
:[[Image:Board-26-Oct-2012-A.jpg|400px]] ''click to enlarge''
:[[Image:Board-26-Oct-2012-B.jpg|400px]] ''click to enlarge''
:[[Image:Board-26-Oct-2012-C.jpg|400px]] ''click to enlarge''
 
== Week 9 ==
 
=== 30 Oct 2012 (09A) ===
We will consider single and multiple co-current extraction.
* [[Media:2012-4M3-class-08E.pdf| Slides for class]]
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-09A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-09A.mp4 video] recording of the class.
* Photo of the board during class
:[[Image:Board-30-Oct-2012.jpg|400px]] ''click to enlarge''
 
=== 01 Nov 2012 (09B) ===


<!-- == Week 5 ==
We should be able to wrap up the section by studying counter-current liquid-liquid extraction.
=== 02 October 2012 (05A) ===
* [[Media:2012-4M3-class-08E.pdf | Slides for class]]  
* We continue to learn more about membrane separations; we will start by overviewing some terminology related to membranes and understanding where membranes are used and why.
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-09B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-09B.mp4 video] recording of the class.
* [[Media:2012-4M3-class-05.pdf | Slides for class]]
* Photo of the board during class
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-05A.mp3 Audio], but unfortunately there is no video available (forgot to turn the camera on). I do have a photo of the white board available:
:[[Image:Board-01-Nove-2012.jpg|400px]] ''click to enlarge''
[[Image:Membrane-topics-2012.jpg | 400px ]] ''click to enlarge''


=== 04 October 2012 (05B) ===
=== 02 Nov 2012 (09C) ===
* We look at microfiltration and applications of it.
* [[Media:2012-4M3-class-08E.pdf | Slides for class]]
* [[Media:2012-4M3-class-05.pdf | Slides for class]] (updated): print from slide 14 to 25
* There will be no formal teaching in class today. You can ask questions about assignment 4, and there will be a tutorial question from assignment 5.
* [http://learnche.mcmaster.ca/media/4M3-2012-Class-05B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2012-05B.mp4 video] recording of the class
* The board from today's class:
[[Image:White-board-04-Oct-2012.jpg|400px]] ''click to enlarge''
-->

Latest revision as of 20:12, 27 November 2012

Class date(s): 23 to 26 October 2012
Download video: Link [102 M]
Download video: Link [123 M]
Download video: Link [127 M]
Download video: Link [119 M]
Download video: Link [119 M]

References

Please use these references to read ahead, or for extra background reading on liquid-liquid extraction. In alphabetical order:

  • Ghosh, R. "Principles of Bioseparations Engineering", Chapter 7, McMaster (reserve)
  • Geankoplis, C.J. "Transport Processes and Separation Process Principles", Chapter 12 in 3rd and 4th edition, McMaster Libraries (reserve)
  • Perry's Chemical Engineers' Handbook, Chapter 15, Direct link (McMaster subscription)
  • Richardson and Harker, "Chemical Engineering, Volume 2", 5th edition, Chapter 13 ebook
  • Schweitzer, "Handbook of Separation Techniques for Chemical Engineers", Chapter 1.9, McMaster library
  • Seader, Henley and Roper, "Separation Process Principles", Chapter 8 in 2nd and 3rd edition McMaster Libraries (reserve)

Interesting applications / Enrichment materials

Acetic-acid-water-ethyl-acetate-flowsheet-Seader-3ed-p300.jpg click to enlarge

Week 8

23 Oct 2012 (08A)

25 Oct 2012 (08B)

26 Oct 2012 (08C)

Board-26-Oct-2012-A.jpg click to enlarge
Board-26-Oct-2012-B.jpg click to enlarge
Board-26-Oct-2012-C.jpg click to enlarge

Week 9

30 Oct 2012 (09A)

We will consider single and multiple co-current extraction.

Board-30-Oct-2012.jpg click to enlarge

01 Nov 2012 (09B)

We should be able to wrap up the section by studying counter-current liquid-liquid extraction.

Board-01-Nove-2012.jpg click to enlarge

02 Nov 2012 (09C)

  • Slides for class
  • There will be no formal teaching in class today. You can ask questions about assignment 4, and there will be a tutorial question from assignment 5.
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