Difference between revisions of "Liquid-liquid extraction - 2013"
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{{ClassSidebar | {{ClassSidebar | ||
| date = 05 November | | date = 05 to 14 November | ||
| dates_alt_text = | | dates_alt_text = | ||
| vimeoID1 = | | vimeoID1 = 78662791 | ||
| vimeoID2 = | | vimeoID2 = 78845789 | ||
| vimeoID3 = | | vimeoID3 = 78937809 | ||
| vimeoID4 = | | vimeoID4 = 79238604 | ||
| vimeoID5 = | | vimeoID5 = 79418024 | ||
| vimeoID6 = | | vimeoID6 = | ||
| vimeoID7 = | | vimeoID7 = | ||
| Line 15: | Line 15: | ||
| assignment_instructions = | | assignment_instructions = | ||
| assignment_solutions = | | assignment_solutions = | ||
| video_download_link_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-10A.mp4 | | video_download_link_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-Class-10A.mp4 | ||
| video_download_link_MP4_size = M | | video_download_link_MP4_size = 310 M | ||
| video_notes1 = | | video_notes1 = | ||
| video_download_link2_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-10B.mp4 | | video_download_link2_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-Class-10B.mp4 | ||
| video_download_link2_MP4_size = M | | video_download_link2_MP4_size = 446 M | ||
| video_notes2 = | | video_notes2 = | ||
| video_download_link3_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-10C.mp4 | | video_download_link3_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-Class-10C.mp4 | ||
| video_download_link3_MP4_size = M | | video_download_link3_MP4_size = 514 M | ||
| video_notes3 = | | video_notes3 = | ||
| video_download_link4_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-11A.mp4 | | video_download_link4_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-Class-11A.mp4 | ||
| video_download_link4_MP4_size = M | | video_download_link4_MP4_size = 161 M | ||
| video_notes4 = | | video_notes4 = | ||
| video_download_link5_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-11B.mp4 | | video_download_link5_MP4 = http://learnche.mcmaster.ca/media/4M3-2013-Class-11B.mp4 | ||
| video_download_link5_MP4_size = M | | video_download_link5_MP4_size = M | ||
| video_notes5 = | | video_notes5 = | ||
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== Interesting applications / Enrichment materials == | == Interesting applications / Enrichment materials == | ||
These first 3 readings seem old, but they are still relevant. For example, the same principles are used in modern bioseparations. | |||
# A comprehensive article on [http://learnche.mcmaster.ca/media/mcmaster/Bailes-Hanson-Hughes--Liquid-liquid-extraction.pdf liquid-liquid extraction] which describes the various units available. | |||
# A [http://learnche.mcmaster.ca/media/mcmaster/Hanson--Solvent-extraction.pdf reading on solvent extraction principles] | |||
# A general article on [http://learnche.mcmaster.ca/media/mcmaster/Reissinger-Schroter--Liquid-liquid-extractors.pdf liquid liquid extractors]. | |||
# An interesting [http://learnche.mcmaster.ca/media/mcmaster/Moore--Using-principles-of-inherent-safety-in-design-of-hydrometallurgical-solvent-extraction-plants.pdf reading on safety in liquid-liquid extraction plants]: a further reason for counter-current operations to minimize solvent use. | |||
# Here's [http://webpages.sdsmt.edu/~ddixon/CBE417_Lec_23_LLE_Draft_3-print.pdf another instructor's slides] on the same topic - sometimes a different point of view helps to understand. | |||
<!-- * The flowsheet for separating acetic acid from water using ethyl acetate solvent. This flowsheet has the mass flow rates, to help contrast it to distillation. | <!-- * The flowsheet for separating acetic acid from water using ethyl acetate solvent. This flowsheet has the mass flow rates, to help contrast it to distillation. | ||
:[[Image:Acetic-acid-water-ethyl-acetate-flowsheet-Seader-3ed-p300.jpg|300px]] <span style="color:#8822AA">''click to enlarge''</span> | :[[Image:Acetic-acid-water-ethyl-acetate-flowsheet-Seader-3ed-p300.jpg|300px]] <span style="color:#8822AA">''click to enlarge''</span> --> | ||
== Class notes == | |||
=== 05 November 2013 (10A) === | |||
* [[Media:2013-4M3-Liquid-Liquid-Extraction.pdf | Slides for class]] | |||
* [http://learnche.mcmaster.ca/media/4M3-2013-Class-10A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2013-Class-10A.mp4 video] recording of the class. | |||
=== 07 November 2013 (10B) === | |||
* [[Media:2013-4M3-Liquid-Liquid-Extraction.pdf | Slides for class]] (slides 24 and onwards are new). Or [[Media:2013-4M3-Liquid-Liquid-Extraction-10B.pdf | just print the new ones]]. | |||
* [http://learnche.mcmaster.ca/media/4M3-2013-Class-10B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2013-Class-10B.mp4 video] recording of the class. | |||
* The [[Media:Seader-ternary-example-base.pdf|ternary diagram used in today's class]]. Download and print it out for practice problems. | |||
=== 08 November 2013 (10C) === | |||
* No new notes; we will complete the notes from 07 November. | |||
* A [http://www.youtube.com/watch?v=n7DPiuHllZE more accurate method to interpolate tie lines] | |||
* [http://learnche.mcmaster.ca/media/4M3-2013-Class-10C.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2013-Class-10C.mp4 video] recording of the class. | |||
== | === 12 November 2013 (11A) === | ||
* [[Media:2013-4M3-Liquid-Liquid-Extraction.pdf | All slides, with full solutions to problems]] (slides 45 and onwards are new). Or [[Media:2013-4M3-Liquid-Liquid-Extraction-11A.pdf | just print the new ones]]. | |||
* [http://learnche.mcmaster.ca/media/4M3-2013-Class-11A.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2013-Class-11A.mp4 video] recording of the class. | |||
=== | === 14 November 2013 (11B) === | ||
* [[ | * No new notes. See notes from 12 November. We will complete this section and start the next section on [[Adsorption_separations_-_2013 | adsorption]]. | ||
* [http://learnche.mcmaster.ca/media/4M3-2013-Class-11B.mp3 Audio] and [http://learnche.mcmaster.ca/media/4M3-2013-Class-11B.mp4 video] recording of the class. | |||
Latest revision as of 21:14, 15 November 2013
| Class date(s): | 05 to 14 November | ||||
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References
Please use these references to read ahead, or for extra background reading on liquid-liquid extraction. In alphabetical order:
- Ghosh, R. "Principles of Bioseparations Engineering", Chapter 7, McMaster (reserve)
- Geankoplis, C.J. "Transport Processes and Separation Process Principles", Chapter 12 in 3rd and 4th edition, McMaster Libraries (reserve)
- Perry's Chemical Engineers' Handbook, Chapter 15, Direct link (McMaster subscription)
- Richardson and Harker, "Chemical Engineering, Volume 2", 5th edition, Chapter 13 ebook
- Schweitzer, "Handbook of Separation Techniques for Chemical Engineers", Chapter 1.9, McMaster library
- Seader, Henley and Roper, "Separation Process Principles", Chapter 8 in 2nd and 3rd edition McMaster Libraries (reserve)
Interesting applications / Enrichment materials
These first 3 readings seem old, but they are still relevant. For example, the same principles are used in modern bioseparations.
- A comprehensive article on liquid-liquid extraction which describes the various units available.
- A reading on solvent extraction principles
- A general article on liquid liquid extractors.
- An interesting reading on safety in liquid-liquid extraction plants: a further reason for counter-current operations to minimize solvent use.
- Here's another instructor's slides on the same topic - sometimes a different point of view helps to understand.
Class notes
05 November 2013 (10A)
- Slides for class
- Audio and video recording of the class.
07 November 2013 (10B)
- Slides for class (slides 24 and onwards are new). Or just print the new ones.
- Audio and video recording of the class.
- The ternary diagram used in today's class. Download and print it out for practice problems.
08 November 2013 (10C)
- No new notes; we will complete the notes from 07 November.
- A more accurate method to interpolate tie lines
- Audio and video recording of the class.
12 November 2013 (11A)
- All slides, with full solutions to problems (slides 45 and onwards are new). Or just print the new ones.
- Audio and video recording of the class.
14 November 2013 (11B)
- No new notes. See notes from 12 November. We will complete this section and start the next section on adsorption.
- Audio and video recording of the class.